Procedure for preparation and standardization 0.1 N Potassium Arsenite

1. OBJECTIVE
To lay down the procedure for preparation and standardization of 0.1 N Potassium Arsenite

2. SCOPE
This procedure is applicable to Quality Control Department

3. RESPONSIBILITY
• Officer QC
• Manager QC

4. SAFETY INSTRUCTIONS
• Proper handling the apparatus.
• Always wear appropriate personal protective equipment when handling this chemical.
• Always handle the chemicals with care and dispose of any waste properly.

5. PROCEDURE
5.1 PREPARATION
5.1.1 Dissolve 4.9455 g of arsenic trioxide primary standard, previously dried at 105 for 1 hour, in 75 mL of 1 N potassium hydroxide.
5.1.2 Add 40 g of potassium bicarbonate, dissolved in about 200 mL of water, and dilute with water to 1000.0 ml.

6. RELATED DOCUMENTS
N/A

7. DISTRIBUTION INDEX
Original Copy will be retained by Quality Assurance Department.

DISTRIBUTION INDEX
Distributed To Copy No. Received By/Date
Quality Control Department 01 ,

8. ABBREVIATIONS
Q.C Quality Control Department
TS Test Solution
Gm Gram
ml Milliliter

9. REVISION HISTORY

Revision No. Issue Date Supersedes Reason of Change / Description
          Revision No.              Dated     
00 10/02/2023 00                            N/A First Version

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